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The production of natural gas hydrates will change the cementation strength, porosity, and effective stress in the stratum, which may lead to engineering and geological disasters. Sand production is a phenomenon where sand particles are carried out of the reservoir along with fluids during gas extraction, posing challenges to safe and sustainable production. This study explored the mechanism of fine particle migration in multiphase flow by a microscopic visualization test device. The device can inject a gas–liquid–solid phase at the same time and allow real-time observation. Experimental tests on fine particle migration of single- and two-phase fluid flow were carried out considering different conditions, i.e., fine particle concentration, fine particle size, fluid flow rate, and gas–liquid ratio. The results show that in single-phase fluid flow, the original gas will gradually dissolve in the liquid phase, and finally stay in the test device as bubbles, which can change the pore structures, resulting in the accumulation of fine particles at the gas–liquid interface. In two-phase fluid flow with mixed gas–water fluids, there are two flow modes of gas–liquid flow: mixed flow and separated flow. The interfacial tension at the gas–liquid interface can effectively migrate fine particles when the gas–liquid flows alternately and the sand production rate further increases as the gas–liquid ratio increases. In addition, changes in the concentration of fine particles, particle size, fluid flow rate, and the gas–liquid ratio will affect the migration of fine particles, leading to differences in the final sand production.
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The degradation of soil bonding, which can be described by the evolution of bond degradation variables, is essential in the constitutive modeling of cemented soils. A degradation variable with a value of 0/1.0 indicates that the applied stress is completely sustained by bonded particles/unbounded grains. The discrete element method (DEM) was used for cemented soils to analyze the bond degradation evolution and to evaluate the degradation variables at the contact scale. Numerical cemented soil samples with different bonding strengths were first prepared using an advanced contact model (CM). Constant stress ratio compression, one-dimensional compression, conventional triaxial tests (CTTs), and true triaxial tests (TTTs) were then implemented for the numerical samples. After that, the numerical results were adopted to investigate the evolution of the bond degradation variables BN and B0. In the triaxial tests, B0 evolves to be near to or larger than BN due to shearing, which indicates that shearing increases the bearing rate of bond contacts. Finally, an approximate stress-path-independent bond degradation variable Bσ was developed. The evolution of Bσ with the equivalent plastic strain can be effectively described by an exponential function and a hyperbolic function.
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The deterioration of anhydrite rock exposed to a freeze–thaw environment is a complex process. Therefore, this paper systematically investigated the physical and mechanical evolutions of freeze–thawed anhydrite rock through a series of multi-scale laboratory tests. Meanwhile, the correlation between pore structure and macroscopic mechanical parameters was discussed, and the deterioration mechanisms of anhydrite rock under freeze–thaw cycles were revealed. The results show that with the increase in freeze–thaw processes, the mechanical strength, elastic modulus, cohesion, proportions of micropores (r ≤ 0.1 μm), and PT-Ipore throat (0–0.1 μm) decrease exponentially. In comparison, the mass variation, proportions of mesopores (0.1 μm < r < 1 μm), macropores (r ≥ 1 μm), and PT-II pore throat (0.1–4 μm) increase exponentially. After 120 cycles, the mean porosity increases by 66.27%, and there is a significant honeycomb and pitted surface phenomenon. Meanwhile, as the freeze–thaw cycles increase, the frost resistance coefficient decreases, while the damage variable increases. The correlation analysis between pore structure and macroscopic mechanical parameters shows that macropores play the most significant role in the mechanical characteristic deterioration of freeze–thawed anhydrite rock. Finally, it is revealed that the water–rock expansion and water dissolution effects play a crucial role in the multi-scale damage of anhydrite rock under the freeze–thaw environment.
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To study the mechanical and cracking modes of anhydrite rock under the freeze–thaw weathering process, the physico-mechanical characteristics and morphology evolutions of anhydrite samples were determined by a series of laboratory tests. Then, a numerical simulation model was established through the PFC2D program, and the types and number of cracks during the uniaxial compression conditions were analyzed. Finally, the distribution of maximum principal stress and shear stress was revealed. The results indicate that as the number of freeze–thaw cycles increases, there is a growth in the mass loss rate and macroscopic damage variables while the uniaxial compression strength and elastic modulus decrease exponentially. Under uniaxial compression stress, the proportion of tensile cracks in the anhydrite model is the highest, followed by tensile shear cracks and compressive shear cracks. As the number of freeze–thaw cycles increases, the proportion of tensile cracks increases exponentially, while the proportion of tensile shear cracks and compressive shear cracks decreases exponentially. Furtherly, it is found that the maximum principal stress and maximum shear stress extreme values decrease exponentially with the increase of freeze–thaw cycles. For example, after 120 cycles, the maximum shear stress at the peak stress point decreased by 47.3%. The research results will promote the comprehension of anhydrite rock geotechnical engineering disaster mechanisms in cold regions.
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Abstract As an in‐depth profile control agent, water‐soluble phenolic resin crosslinking polyacrylamide weak gel has been widely used in the middle and high water cut stage of water flooding reservoir. In this study, the phenolic resin was synthesized by two‐step alkali catalysis. Factors influencing the synthesis of phenolic resin, including the molar ratio of phenol and formaldehyde, catalyst types, reaction time, were investigated with hydroxylmethyl and aldehyde content as the criterion. When the molar ratio of phenolic resin was 1:2 and NaOH was catalyst, at 80°C for 4 h, the phenolic resin had the highest hydroxymethyl content (49.37%) and the lowest free aldehyde content (2.95%). Weak gel was formed by the reaction of LT002‐polyacrylamide with phenolic resin. Taking the gelation time and strength as criteria, the factors influencing the crosslinking property, including hydroxymethyl content, crosslinker addition, and polyacrylamide concentration were investigated respectively. Under optimal formulation, the property investigation shows that the hydroxymethyl group in the phenolic resin can be crosslinked with the amide group in polyacrylamide, the gelation time is long (50–60 h), and the gelation strength is larger than 5 × 10 4 mPa s, which is conductive to the plugging of deep oil layers. When the permeability was 5061 × 10 −3 μm 2 , the plugging rate was 72.73%.